Art
J-GLOBAL ID:200902126742392215   Reference number:02A0270613

Solvent-Free One-Pot Reduction of Imines Generated in situ from Aldehydes and Aniline by Tributyltin Hydride on Silica Gel.

シリカゲル上でのトリブチルすずヒドリドによりアルデヒドとアニリンからin situで発生させたイミンの無溶媒ワンポット還元
Author (3):
Material:
Issue:Page: 274-275  Publication year: Mar. 05, 2002 
JST Material Number: S0742A  ISSN: 0366-7022  CODEN: CMLTAG  Document type: Article
Article type: 短報  Country of issue: Japan (JPN)  Language: ENGLISH (EN)
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JST classification (3):
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Aromatic monocyclic aldehydes  ,  Aromatic monocyclic amine,imine,quaternary ammonium,immonium compounds  ,  Oxidation,reduction 
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Reference (31):
  • 1) R. O. Hutchins and M. K. Hutchins, in “Comprehensive Organic Synthesis,” ed. by B. M. Trost and I. Fleming, Pergamon, Oxford (1991), Vol. 8, p 25.
  • 2) a) R. F. Borch, M. D. Bernstein, and H. D. Durst, J. Am. Chem. Soc., 93, 2897 (1971).
  •  b) C. F. Lane, Synthesis, 1975, 135.
  •  c) A. F. Abdel-Magid, K. G. Carson, B. D. Harris, C. A. Maryanoff, and R. D. Shah, J. Org. Chem., 61, 3849 (1996).
  •  d) R. J. Mattson, K. M. Pham, D. J. Leuck, and K. A. Cowen, J. Org. Chem., 55, 2552 (1990).
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