Art

J-GLOBAL ID：200902272377491361   Reference number：03A0386631

Atropisomers of 1-(Acyl or Aroyl)-2-naphthylindolines. Isolation, X-Ray Crystal Structure and Conformational Analysis

1-(アシルまたはアロイル)-2-ナフチルインドリン類のアトロプ異性体 単離,X線結晶構造及び配座解析

Author (6)： ITO F (Kumamoto Univ., Kumamoto, JPN) ,  MORIGUCHI T (Kumamoto Univ., Kumamoto, JPN) ,  YOSHITAKE Y (Kumamoto Univ., Kumamoto, JPN) ,  ETO M (Kumamoto Univ., Kumamoto, JPN) ,  YAHARA S (Kumamoto Univ., Kumamoto, JPN) ,  HARANO K (Kumamoto Univ., Kumamoto, JPN)
Material： Chemical and Pharmaceutical Bulletin  (Chemical & Pharmaceutical Bulletin)
Volume： 51  Issue： 6  Page： 688-696  Publication year： Jun. 01, 2003 
JST Material Number： G0504A  ISSN： 0009-2363  CODEN： CPBTAL  Document type： Article
Article type： 原著論文  Country of issue： Japan (JPN)  Language： ENGLISH (EN)

Thesaurus term： *nitrogen heterocyclic compound ,...
Semi thesaurus term： hindered rotation

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JST classification (2)： Condensed derivatives of pyrroles  (CF07077C) ,  Experimental research on molecular structure and properties  (CB01020I)

Substance index (28)： (4-Nitrophenyl)(2α-hydroxy-3,3-dimethylindoline-1-yl) ketone ,  (4-Chlorophenyl)(2α-hydroxy-3,3-dimethylindoline-1-yl) ketone ,  Phenyl(2α-hydroxy-3,3-dimethylindoline-1-yl) ketone ,  4-Methylphenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  4-Methoxyphenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  4-(Dimethylamino)phenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  3-Nitrophenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  3-Methylphenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  3-Methoxyphenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  (3,5-Dinitrophenyl)(2α-hydroxy-3,3-dimethylindoline-1-yl) ketone ,  3,5-Dimethylphenyl[(2R)-2α-hydroxy-3,3-dimethyl-1-indolinyl] ketone ,  1-(2α-Hydroxy-3,3-dimethylindoline-1-yl)ethanone ,  1-[(2R)-2α-Hydroxy-3,3-dimethyl-1-indolinyl]-1-propanone ,  1-[(2R)-2α-Hydroxy-3,3-dimethyl-1-indolinyl]-1-butanone ,  1-[(2S)-1-(4-Nitrobenzoyl)-3,3-dimethylindoline-2α-yl]-2-naphthol ,  1-[(2S)-1-(4-Chlorobenzoyl)-3,3-dimethylindoline-2α-yl]-2-naphthol ,  Phenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  4-Methylphenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  4-Methoxyphenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  4-(Dimethylamino)phenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  (3-Nitrophenyl)[2α-(2-hydroxy-1-naphthyl)-3,3-dimethylindoline-1-yl] ketone ,  1-[1-(3-Methylbenzoyl)-3,3-dimethylindoline-2α-yl]-2-naphthol ,  3-Methoxyphenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  3,5-Dinitrophenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  3,5-Dimethylphenyl[(2S)-2α-(2-hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl] ketone ,  1-[(2S)-2α-(2-Hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl]ethanone ,  1-[(2S)-2α-(2-Hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl]-1-propanone ,  1-[(2S)-2α-(2-Hydroxy-1-naphthyl)-3,3-dimethyl-1-indolinyl]-1-butanone

Reference (40)：

• 1) Present address: School of Agriculture, Kyushu Tokai University, 5435 Kawayo, Choyoson, Asogun, Kumamoto 869–1404, Japan.
• 2) Oki M., Angew. Chem., 88, 67—74 (1976).
• 3) Oki M., “Topics in Stereochemistry,” Vol. 14, ed. by Allinger N. L., Eliel E. L., Wilen S. H., John Wiley & Sons Inc., New York, 1983, pp. 47—79.
• 4) Oki M., Acc. Chem. Res., 23, 351—356 (1990).
• 5) Randall W. C., Anderson P. S., Cresson E. L., Hunt C. A., Lyon T. F., Rittle K. E., Remy D. C., Springer J. P., Hirshfield J. M., Hoogsteen K., Williams M., Risley E. A., Tataro J. A., J. Med. Chem., 22, 1222—1230 (1979).

Terms in the title (6)： アロイル ,  アトロプ異性体 ,  単離 ,  X線 ,  結晶構造 ,  配座解析