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J-GLOBAL ID：200902160509374227   Reference number：02A0470841

Synthesis of 1,2-Dihydrobenz[c]azepin-3-one via Acid-catalyzed Cyclization of N-Arylmethyl-N-methyl-3-phenylsulfanylacrylamide.

N-アリールメチル-N-メチル-3-フェニルスルファニルアクリルアミドの酸接触環化を経由する1,2-ジヒドロベンゾ[c]アゼピン-3-オンの合成

Author (7)： HORIGUCHI Y (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  SAITOH T (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  KASHIWAGI T (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  KATURA L (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  ITAGAKI M (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  TODA J (Showa Coll. Pharmaceutical Sci., Tokyo, JPN) ,  SANO T (Showa Coll. Pharmaceutical Sci., Tokyo, JPN)
Material： Heterocycles  (International Journal for Reviews and Communications in Heterocyclic Chemistry)
Volume： 57  Issue： 6  Page： 1063-1077  Publication year： Jun. 01, 2002 
JST Material Number： S0966A  ISSN： 0385-5414  CODEN： HTCYAM  Document type： Article
Article type： 原著論文  Country of issue： Japan (JPN)  Language： ENGLISH (EN)

Thesaurus term： chemical synthesis ,...

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JST classification (2)： Seven-membered heterocyclic compounds  (CF07110I) ,  Structure effect on organic reaction  (CF02110Z)

Substance index (20)： p-Toluenesulfonic acid ,  (E)-N-Methyl-3-(phenylthio)acrylamide ,  (Z)-N-Benzyl-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(2-Methoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(4-Methoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(3-Methoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(3,5-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (E)-N-(3,5-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(2,3-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (E)-N-(2,3-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(3,4-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (E)-N-(3,4-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(2,5-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (Z)-N-(2,4-Dimethoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  (E)-N-Benzyl-N-methyl-3-(phenylthio)acrylamide ,  (E)-N-(2-Methoxybenzyl)-N-methyl-3-(phenylthio)acrylamide ,  1,2-Dihydro-2-methyl-8-methoxy-3H-2-benzazepine-3-one ,  1,2-Dihydro-2-methyl-6-methoxy-3H-2-benzazepine-3-one ,  1,2-Dihydro-2-methyl-6,8-dimethoxy-3H-2-benzazepine-3-one ,  1,2-Dihydro-2-methyl-8,9-dimethoxy-3H-2-benzazepine-3-one

Terms in the title (2)： 酸 ,  環化