Art

J-GLOBAL ID：200902274673746203   Reference number：09A1282555

Preparation of New Nitrogen-Bridged Heterocycles 67. Syntheses of α,α′-Bis[(thieno[3,4-b]indolizin-3-yl)thio]-o-, m-, and p-xylene Derivatives and Their Conformational Structures

新しい窒素架橋複素環化合物の合成 67.α,α′-ビス[(チエノ[3,4-b]インドリジン-3-イル)チオ]-o-,m-,およびp-キシレン誘導体の合成とその立体配座構造

Author (7)： KAKEHI Akikazu (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  SUGA Hiroyuki (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  OKUMURA Yukihisa (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  SHINOHARA Masatoshi (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  KAKO Tomonao (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  SEKIGUCHI Takeshi (Dep. of Chemistry and Material Engineering, Fac. of Engineering, Shinshu Univ.) ,  SHIRO Motoo (Rigaku X-Ray Res. Lab., Rigaku Corp.)
Material： Chemical and Pharmaceutical Bulletin  (Chemical & Pharmaceutical Bulletin)
Volume： 57  Issue： 12  Page： 1385-1390 (J-STAGE)  Publication year： 2009 
JST Material Number： G0504A  ISSN： 0009-2363  CODEN： CPBTAL  Document type： Article
Article type： 原著論文  Country of issue： Japan (JPN)  Language： ENGLISH (EN)

Thesaurus term： *nitrogen heterocyclic compound ,  sulfur heterocyclic compound ,  *sulfide (organic) ,  chemical synthesis ,  Alkylation ,  cyclization reaction ,  dehalogenation ,  *steric conformation ,  proton magnetic resonance ,  crystal structure

JST classification (2)： Other condensed derivatives of pyridine  (CF07097Y) ,  Crystal structure of heterocyclic compounds  (BK08030Q)

Substance index (10)： 1,2-Bis(dibromomethyl)benzene ,  1,4-Bis(dibromomethyl)benzene ,  2-(4-Bromobenzoyl)-4-pyridinio-5-thiolatothiophene-3-acetic acid ethyl ester ,  2-Benzoyl-4-(3,5-dimethylpyridinio)-5-thiolatothiophene-3-acetic acid ethyl ester ,  3,3′-[1,2-Phenylenebis(methylenethio)]bis[1-(4-bromobenzoyl)-2-thia-3b-azacyclopenta[a]indene-8-carboxylic acid ethyl] ester ,  3,3′-[1,2-Phenylenebis(methylenethio)]bis(1-benzoyl-5,7-dimethyl-2-thia-3b-azacyclopenta[a]indene-8-carboxylic acid ethyl) ester ,  2-(4-Bromobenzoyl)-4-(3,5-dimethylpyridinio)-5-thiolatothiophene-3-acetic acid ethyl ester ,  1,3-Bis(bromomethyl)benzene ,  3,3′-[1,3-Phenylenebis(methylenethio)]bis(1-benzoyl-5,7-dimethyl-2-thia-3b-azacyclopenta[a]indene-8-carboxylic acid ethyl) ester ,  3,3′-[1,3-Phenylenebis(methylenethio)]bis[1-(4-bromobenzoyl)-5,7-dimethyl-2-thia-3b-azacyclopenta[a]indene-8-carboxylic acid ethyl] ester

Reference (18)：

• 1) For part 66 of this series, see Abe T., Okumura Y., Suga H., Kakehi A., Heterocycles, in press.
• 2) Jones G. B., Tetrahedron, 57, 7999—8016 (2001).
• 3) Meyer E. A., Castellano R. K., Diederich F., Angew. Chem. Int. Ed., 42, 1210—1250 (2003).
• 4) Yamada S., Yuki Gosei Kagaku Kyokaishi, 63, 339—350 (2003).
• 5) Carroll W. R., Pellechia P., Shimizu K. D., Org. Lett., 10, 3547—3550 (2008).

Terms in the title (8)： 窒素 ,  架橋 ,  複素環化合物の合成 ,  ビス ,  インドリジン ,  p-キシレン ,  誘導体 ,  立体配座