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J-GLOBAL ID：200902294332746320   Reference number：03A0710544

The First Total Synthesis of Discorhabdin A.

ジスコルハブジンAの最初の全合成

Author (7)： TOHMA H (Osaka Univ., Osaka, JPN) ,  HARAYAMA Y (Osaka Univ., Osaka, JPN) ,  HASHIZUME M (Osaka Univ., Osaka, JPN) ,  IWATA M (Osaka Univ., Osaka, JPN) ,  KIYONO Y (Osaka Univ., Osaka, JPN) ,  EGI M (Osaka Univ., Osaka, JPN) ,  KITA Y (Osaka Univ., Osaka, JPN)
Material： Journal of the American Chemical Society  (J Am Chem Soc)
Volume： 125  Issue： 37  Page： 11235-11240  Publication year： Sep. 17, 2003 
JST Material Number： C0254A  ISSN： 0002-7863  CODEN： JACSAT  Document type： Article
Article type： 原著論文  Country of issue： United States (USA)  Language： ENGLISH (EN)

Thesaurus term： total synthesis ,...
Semi thesaurus term： bridged compound ,...

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JST classification (1)： Alkaloids  (CF10030D)

Substance index (19)： PIFA ,  (+)-Discorhabdin A ,  Makaluvamine F ,  L-Tyrosine methyl ,  N-(1,4-Dioxo-1,4-dihydronaphthalene-2-yl)-L-tyrosine methyl ester ,  2-Methoxy-2,3,5,10-tetrahydrospiro[benzo[g]quinoline-4(1H),1′-[2,5]cyclohexadiene]-4′,5,10-trione ,  2-(Acetylthio)-2,3,5,10-tetrahydrospiro[benzo[g]quinoline-4(1H),1′-[2,5]cyclohexadiene]-4′,5,10-trione ,  2-(4-Methoxybenzylthio)-2,3,5,10-tetrahydrospiro[benzo[g]quinoline-4(1H),1′-[2,5]cyclohexadiene]-4′,5,10-trione ,  N-Trityl-3-bromo-L-tyrosine methyl ester ,  2-Bromo-4-[(S)-2-(tritylamino)-3-(tert-butyldimethylsiloxy)propyl]phenol ,  1-Tosyl-7-[[(αS)-α-(tert-butyldimethylsiloxymethyl)-3-bromo-4-hydroxyphenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  (8S)-3′-Bromo-5-tosyl-8α-(tert-butyldimethylsiloxymethyl)-2,3,5,6,7,8-hexahydrospiro[pyrrolo[4,3,2-de][1,7]phenanthroline-10(9H),1′-[2,5]cyclohexadiene]-4′,6-dione ,  (6′S,10S)-5-Tosyl-5′-bromo-6′β,8α-epoxy-2,3,5,6,7,8-hexahydrospiro[pyrrolo[4,3,2-de][1,7]phenanthroline-10(9H),1′-[2]cyclohexene]-4′,6-dione ,  1-Tosyl-7-[[(αS)-α-(triisopropylsiloxymethyl)-3-bromo-4-hydroxyphenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  1-Tosyl-7-[[(αS)-α-(tert-butyldiphenylsiloxymethyl)-3-bromo-4-hydroxyphenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  1-Tosyl-7-[[(αS)-α-(tert-butyldimethylsiloxymethyl)-3-bromo-4-(trimethylsiloxy)phenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  1-Tosyl-7-[[(αS)-α-(tert-butyldimethylsiloxymethyl)-3-bromo-4-(tert-butyldimethylsiloxy)phenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  1-Tosyl-7-[[(αS)-α-(tert-butyldimethylsiloxymethyl)-3-bromo-4-(triisopropylsiloxy)phenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one ,  1-Tosyl-7-[[(αS)-α-(tert-butyldimethylsiloxymethyl)-3-bromo-4-(tert-butyldiphenylsiloxy)phenethyl]amino]-1,3,4,8-tetrahydropyrrolo[4,3,2-de]quinoline-8-one

Terms in the title (2)： ジスコルハブジンA ,  全合成