Art

J-GLOBAL ID：201702271838321429   Reference number：17A1079312

Simultaneous determination of primary and secondary D- and L-amino acids by reversed-phase high-performance liquid chromatography using pre-column derivation with two-step labelling method

二段階標識法によるプレカラム誘導体化を用いた逆相高速液体クロマトグラフィーによる第一級および第二級のD-およびL-アミノ酸の同時定量

Author (4)： YOKOYAMA Takehiko (Kitasato Univ., Sagamihara, JPN) ,  TOKUDA Masaharu (Fisheries Res. and Education Agency, Minami-ise, JPN) ,  AMANO Masafumi (Kitasato Univ., Sagamihara, JPN) ,  MIKAMI Koji (Hokkaido Univ., Hakodate, JPN)
Material： Bioscience, Biotechnology, and Biochemistry  (Bioscience Biotechnology & Biochemistry)
Volume： 81  Issue： 9  Page： 1681-1686  Publication year： Sep. 2017 
JST Material Number： G0021A  ISSN： 0916-8451  CODEN： BBBIEJ  Document type： Article
Article type： 原著論文  Country of issue： United Kingdom (GBR)  Language： ENGLISH (EN)

Thesaurus term： *amino acid ,  simultaneous determination ,  *reversed-phase HPLC ,  *derivatization ,  *diastereomer ,  fluorescent labeling ,  primary amine ,  secondary amine ,  fatty acid ,  aliphatic amine ,  thiol ,  carboxamide ,  sulfur containing amino acid ,  aromatic aldehyde
Semi thesaurus term： *D-amino acid ,  L-aminoacid ,  *precolumn derivatization

JST classification (2)： Amino acids  (CF10070V) ,  Liquid chromatography  (CC04014L)

Substance index (4)： D-Proline ,  Acetylcysteine ,  o-Phthalaldehyde ,  FLEC

Reference (13)：

• Konno R, Brückner H, D’Aniello A, et al., editors. d-Amino acids: a new frontier in amino acids and protein research-practical methods and protocols. New York (NY): Nova Science; 2007.
• Aswad DW. Determination of d- and l-aspartate in amino acid mixtures by high-performance liquid chromatography after derivatization with a chiral adduct of o-phthaldialdehyde. Anal Biochem. 1984;137:405-409.
• Nimura N, Kinoshita T. o-Phthalaldehyde-N-acetyl-L-cysteine as a chiral derivatization reagent for liquid chromatographic optical resolution of amino acid ernantiomers and its application to conventional amino acid analysis. J Chromatogr. 1986;352:169-177.
• Buck RH, Krummen K. Resolution of amino acid enantiomers by high-performance liquid chromatography using automated pre-column derivatisation with a chiral reagent. J Chromatogr. 1984;315:279-285.
• Hashimoto A. Determination of free amino acid enantiomers in rat brain and serum by high-performance liquid chromatography after derivatization with N-tert.-butyloxycarbonyl-l-cysteine and o-phthaldialdehyde. J Chromatogr. 1992;582:41-48.

Terms in the title (6)： 段階 ,  標識法 ,  プレカラム誘導体化 ,  逆相高速液体クロマトグラフィー ,  L-アミノ酸 ,  同時定量